                            INSTRUMENT CONTROL PARAMETERS:    GC-MS
                            ---------------------------------------

   C:\MSDCHEM\1\METHODS\FAME-RBF-24-SAMP.M
      Tue Aug 12 13:18:17 2014

Control Information
------- -----------

Sample Inlet      :  GC
Injection Source  :  GC ALS
Mass Spectrometer :  Enabled


 No Sample Prep method has been assigned to this method.

=============================================================================
                                6890 GC METHOD
=============================================================================


OVEN
   Initial temp:  64 'C (On)               Maximum temp:  240 'C
   Initial time:  1.00 min                 Equilibration time:  2.00 min
   Ramps:
      #  Rate  Final temp  Final time
      1 33.00      196        0.00
      2  4.00      240        7.00
      3   0.0(Off)
   Post temp:  64 'C
   Post time:  1.00 min
   Run time:  23.00 min


FRONT INLET (SPLIT/SPLITLESS)           BACK INLET (SPLIT/SPLITLESS)
   Mode:  Splitless                        Mode:  Splitless
   Initial temp:  230 'C (On)              Initial temp:  240 'C (On)
   Pressure:  14.75 psi (On)               Pressure:  2.00 psi (On)
   Purge flow:  15.0 mL/min                Purge flow:  31.9 mL/min
   Purge time:  1.00 min                   Purge time:  0.00 min
   Total flow:  18.8 mL/min                Total flow:  35.0 mL/min
   Gas saver:  On                          Gas saver:  Off
   Saver flow:  15.0 mL/min                Gas type:  Helium
   Saver time:  3.00 min
   Gas type:  Helium


COLUMN 1                                COLUMN 2
   Capillary Column                        Capillary Column
   Model Number:  Agilent 222-2932LTM      Model Number:  Agilent 222-2932LTM
   DB-225ms (G3900-63023)                  DB-225ms (G3900-63023)
   Max temperature:  240 'C                Max temperature:  240 'C
   Nominal length:  30.0 m                 Nominal length:  30.0 m
   Nominal diameter:  250.00 um            Nominal diameter:  250.00 um
   Nominal film thickness:  0.25 um        Nominal film thickness:  0.25 um
   Mode:  ramped flow                      Mode:  ramped pressure
   Initial flow:  1.1 mL/min               Initial pressure:  2.00 psi
   Initial time:  12.00 min                Initial time:  17.00 min
      #  Rate  Final flow  Final time         #  Rate  Final pres  Final time
      1  0.20      2.1         0.00           1 30.00    32.00         5.00
      2  2.00      0.1         5.00           2   0.0(Off)
      3  2.00      2.1        22.00        Post pressure:  2.00 psi
   Post flow:  1.1 mL/min                  Nominal initial flow:  0.1 mL/min
   Nominal init pressure:  14.76 psi       Average velocity:  4 cm/sec
   Average velocity:  26 cm/sec            Inlet:  Back Inlet
   Inlet:  Front Inlet                     Outlet:  MSD
   Outlet:  MSD                            Outlet pressure:  ambient
   Outlet pressure:  2.00 psi


FRONT DETECTOR (FID)                    BACK DETECTOR (NO DET)
   Temperature:  250 'C (Off)
   Hydrogen flow:  40.0 mL/min (Off)
   Air flow:  450.0 mL/min (Off)
   Mode:  Constant makeup flow
   Makeup flow:  45.0 mL/min (Off)
   Makeup Gas Type: Helium
   Flame:  Off
   Electrometer:  Off
   Lit offset:  2.0


SIGNAL 1                                SIGNAL 2
   Data rate:  20 Hz                       Data rate:  20 Hz
   Type:  test plot                        Type:  test plot
   Save Data:  Off                         Save Data:  Off
   Zero:  0.0 (Off)                        Zero:  0.0 (Off)
   Range:  0                               Range:  0
   Fast Peaks:  Off                        Fast Peaks:  Off
   Attenuation:  0                         Attenuation:  0


COLUMN COMP 1                           COLUMN COMP 2
   (No Detectors Installed)                (No Detectors Installed)


THERMAL AUX 2                           AUX PRESSURE 3
   Use:  MSD Transfer Line Heater          Description:
   Description:                            Gas Type:  Helium
   Initial temp:  240 'C (On)              Initial pressure:  0.00 psi (Off)
   Initial time:  0.00 min
      #  Rate  Final temp  Final time
      1   0.0(Off)


AUX PRESSURE 4                          AUX PRESSURE 5
   Description:                            Description:
   Gas Type:  Helium                       Gas Type:  Helium
   Initial pressure:  0.00 psi (Off)       Initial pressure:  0.00 psi (Off)


VALVES                                  POST RUN
   Valve 5  Switching Off                  Post Time: 1.00 min
      Description:                         Oven Temperature: 64 'C
                                           Column 1 Flow: 1.1 mL/min
                                           Column 2 Pressure: 2.0 psi


TIME TABLE
   Time       Specifier                     Parameter & Setpoint




                               GC Injector


     Front Injector:
        Sample Washes                 0
        Sample Pumps                  3
        Injection Volume           2.00 microliters
        Syringe Size               10.0 microliters
        PreInj Solvent A Washes       0
        PreInj Solvent B Washes       0
        PostInj Solvent A Washes      4
        PostInj Solvent B Washes      3
        Viscosity Delay               1 seconds
        Plunger Speed              Fast
        PreInjection Dwell         0.02 minutes
        PostInjection Dwell        0.02 minutes


     Back Injector:
No parameters specified

 Column 1 Inventory Number : AB002
 Column 2 Inventory Number : AB002

                                MS ACQUISITION PARAMETERS


General Information
------- -----------

Tune File                : atune.u
Acquistion Mode          : Scan/SIM


MS Information
-- -----------

Solvent Delay            : 3.50 min

EMV Mode                 : Relative
Relative Voltage         : 0
Resulting EM Voltage     : 2706

[Scan Parameters]

Low Mass                 : 50.0
High Mass                : 400.0
Threshold                : 10
Sample #                 : 0       A/D Samples    1
[Sim Parameters]

GROUP 1
Group ID                 : All FAMES
Resolution               : Low
Plot 1 Ion               : 67.10
Ions/Dwell In Group      (  Mass,  Dwell) (  Mass,  Dwell) (  Mass,  Dwell) 
                         ( 67.10,     15) ( 74.10,     15) ( 77.10,     15) 
                         ( 79.10,     15) (368.35,     15) 

[MSZones]

MS Source                : 230 C   maximum 350 C
MS Quad                  : 150 C   maximum 200 C


                             END OF MS ACQUISITION PARAMETERS


                              TUNE PARAMETERS for SN: US10481367
                        -----------------------------

 Trace Ion Detection is OFF.

 EMISSION    :      14.833
 ENERGY      :      69.922
 REPELLER    :      22.416
 IONFOCUS    :      82.565
 ENTRANCE_LE :       4.000
 EMVOLTS     :    2705.882
                               Actual EMV  :    2705.88
                               GAIN FACTOR :       9.09
 AMUGAIN     :    2017.000
 AMUOFFSET   :     129.000
 FILAMENT    :       2.000
 DCPOLARITY  :       0.000
 ENTLENSOFFS :      21.082
 MASSGAIN    :     296.000   
 MASSOFFSET  :     -13.000   

                           END OF TUNE PARAMETERS
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                             END OF INSTRUMENT CONTROL PARAMETERS
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